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By Ian D. Wilson

Bioanalytical Separations is quantity four of the multi-volume sequence, instruction manual of Analytical Separations, offering experiences of analytical separation tools and strategies used for the decision of analytes throughout an entire diversity of functions. The subject matter for this quantity is bioanalysis, thus in particular which means the research of substances and their metabolites in organic fluids.

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The desorption device is directly coupled to the detector. P6rbs and co-authors [ 139] coupled HS/SPME directly to MS by thermal desorption and a short GC transfer-line for the determination of volatiles in cheese using only 10 min. sorption. A typical desorption profile of HS/SPME-MS is shown in Fig. 11. Orzechowska et al. [140] determined cocaine by direct coupling of HS/SPME with ion mobility spectrometry. Camitine, an essential factor in the fatty acid metabolism of organisms, was determined by SPMEESI/MS [134].

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