By Adimurthi, Grossi M.
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Extra info for Asymptotic estimates for a two dimensional problem with polynomial nonlinearity
L. Stucky, Inorg. Nucl. Chem. , I , 85 (1965). C. R. D. Thesis, The Ohio State University, 1971. E. B. Fleischer and S. W. Hawkinson,Inorg. , 7, 2312 (1968). E. Ochiai and D. H. Busch, Inorg. , 8, 1798 (1969). K. L. Long and D. H. Busch,Inorg. , 9, 505 (1970). E. Ochiai and D. H. Busch, Chem. , 1968, 905. E. Ochiai, K. M. Long, C. R. Sperati, and D. H. Busch, J. Am. Chem. , 91, 3201 (1969). K. Farmery and D. €1. Busch, Chem. , 1970, 1091; Inorg. , 1 1 , 2901 (1972). L Ochiai and D. H. Busch, Inerg.
J. C. Dabrowiak, F. V. Lovecchio, V. L. Goedken, and D. H. Busch, J. Am. Chem. , 94,5502 (1972). 7. R. A. D. Wentworth and T. S . , 4, 709 (1965). 3. 11- HEPTADECA-1(17),2,11,13,15PENTAENE (2,6-Me214]-1,3,6-triene-1,4,7,1 l-N4) COMPLEXES 2’,6’:3,5-Pyo[ Submitted by A. MARTIN TAIT* and DARYLE H. BUSCH* Checked by J. WILSHIRE’ and A. B. P. LEVER? ’ As is often the case with Schiff-base condensations of the type, the addition of a small amount of acid catalyzes the reaction. 2-4 *Department of Chemistry The Ohio State University, Columbus, OH 43210.
Chemistry Department, Victoria University of Wellington, Wellington, New Zealand. $(1) The analogous tetrafluoroborate salt is prepared in a similar m a n n e ~ ,using ~ 30% tetrafluoroboric acid [hydrogen tetrafluoroborate( 1-)] in place of trifluoromethanesulfonic acid. ' This material reverts to the purple acetonitrile adduct upon exposure t o acetonitrile. 'd §Acetonitrile was dried over molecular sieves and then distilled from CaH, under nitrogen after reflux for 1 hour under nitrogen. Tetrahydrofuran was dried over KOH and then refluxed over and distilled from CaH, under nitrogen.